AMX DAS-M-0608 manuals

Amx DAS-M-0608 User Manual (2 pages)

Brand: Amx | Category: Software | Size: 0.36 MB |

German

English

Table of contents

Type AMX

1

Type LBD

1

Type LBS

1

3,0 3" 91 - 400 ZD 75

2

Amx DAS-M-0608 User Manual (168 pages)

Brand: Amx | Category: Software | Size: 4.97 MB |

German

Table of contents

Cyclometallierung

1

Chemistry

2

NMR-Spektrometer

3

Arbeitsgruppe

3

Lösungsansätze

4

Stickstoffreagenzien

5

Kupfer(n)rhodanid

7

(Übergangs-)

10

("\

11

Einführung

12

Heterocyclen

13

2,6-Dichlor-3-methyl-anilin

14

^-C—C—OR

15

Bedingungen

16

Umsetzung

16

Ks"—p^-Js

17

Y--.^-C0

18

-c,-p^n/

19

Kupfer(I)

20

Triphenylphosphin

20

[f^'V^N^

21

Palladium(IV)-Komplex

22

<>

23

Alkoxygruppe

24

Mahapatra

24

Verbindungen

24

Schwefelreagenzien

24

-CH(CH3)2

25

Übergang

26

Bedingungen:

27

Trimethylphosphat

27

Kaliumjodid

27

N,N-Dimethyl-o-toluidin

27

Formylgruppe

28

'H-NMR-Spektren

29

Gemische

30

'H-NMR-Spektrum

32

"*"

32

Angesichts

33

Experimente

33

-Komplexe

34

Pd^CNEt^

35

1H-NMR-Spektrum

36

1,2-Bis-p-tolylthio-ethan

37

Umsetzungen

38

^Sv^N~^

39

NCS^>2

40

^-NMR-Spektrum

41

AcO^>2

43

HjN—NH3+C1"

44

1,2-Bis-diphenyl

45

^-NMR-Spektroskopie

46

,^Pj>

47

3,3'-Dimethylazobenzol

48

Diplomarbeiten

48

""xXf

49

"XX

50

Trifluoressigsäure/

51

><

52

Cydopalladierung

53

JH-NMR-Spektrum

54

Triethylamin

55

"XC

56

Trifluoressigsäure

57

Dimethylamid

58

Carboxylgruppe

58

Phosphoroxy

59

Synthese

60

^-NMR-Spek

61

13C-NMR-Spektrum

62

Biphenyl

63

Methoxy-Verbindung

64

Methoxy-tris-(p-dimethyl

64

Kupfer(II)

66

NH3-Lösung

66

Hydroxy-Verbindung

69

Temperatur

70

Lithiumdiisopropylamid

71

Ciba-Geigy

71

»C-NMR-Spektren

73

^-NMR-Spektren

73

13C-NMR-Spektren

73

Basispeaks

74

Flash-Chromatographie

74

Rohprodukt

75

Rotationsverdampfer

76

Trennung

78

(DMSO-Ö6

81

Methylenchlo¬

82

Kupfer(II)acetat

82

Verbindung

83

(Kieselgel

83

Hydrolysepro¬

83

Diethyl

84

H2N^^"

85

CO'

86

14KM*"

87

Säulenchromatographie

87

^Pd'°

89

\—N(Et)2

90

(IR-Spektrum

91

Chromatographien

94

Methylgruppe:

98

'S

100

Komplexes

100

Badtemperatur)

101

(liquid):

101

183(17)

102

(CDCI3,200

102

Palladium-Komplexes

103

Phosphin-Palladium-Komplex)

103

Übereinstimmung

105

Derivatisierung

106

Butyllithium

106

Methylenchlorid

107

(-CO-CH3);

108

10%-iger

109

Acetanhydrid

110

Einengen

110

169(M+,14)

111

Cyclopalladierungen

112

"XXX

113

CFsCOO^*

114

"YYY

116

Kieselgel

117

Methylenchlorid/EtOH

120

Azoverbindung

121

Natriumtetrachloropalladat

122

Eisessig

123

Suspension

124

Reaktionslösung

126

Pdladium-Komplexes

128

Benzylpentacarbonylmangan(I)

129

Natronlauge

130

177(M+,100)

131

(CDC13,200

132

(-N(CH3)2);

132

-N(CH3)2);

133

Referenzspektrum

134

Untersuchungen

135

Methoxy

136

Niederschlag

137

Palladium-Komplex

137

Kristallviolett

139

Anschliessend

139

(DMSO-d6,300

141

N(CH3)2);

141

Natriumperoxid

142

Ethylendiamin-Lösung

143

Überführung

144

Methoxy-Kristallviolett

145

Synthesis

146

LeBorgne

147

Moravskiy

148

Compounds

149

Crystallogr

149

Spagnolo

149

Organometallic

150

Springer-Verlag

150

Anorganischen

150

CC"

151

H-^-fjy^y

152

N-Acetyl-o-toluidin

153

N-Trimethylsilyl-o-toluidin

153

-"V"

154

3-Acetyl-2-imino-benzothiazol

155

Hic^y^ymi

156

^C^^N^A^A^

157

CFsCOO^z

158

-%A>AC„

159

N,N-Dimethylanilin

160

4-Dimethylaminobenzaldehyd

160

2-(p-Dimethylaminobenzoyl)-5

160

(\T\eW~-a/~~\

161

5-dimethylaminophenol

162

(p-dimethylaminophenyl)

163

1,2-bis-p-tolylthio-ethane

166

Mangan(I)-Kom

168

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